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The performance of radar absorption of MnxFe3–xO4/rGO nanocomposites prepared from iron sand beach and coconut shell waste
AIMS Materials Science 2023, 10(2): 227-248
Published: 15 April 2023
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In this work, the Fe3O4 nanoparticles from natural iron sand were doped with Mn and combined with reduced-graphene oxide (rGO) to obtain MnxFe3–xO4/rGO nanocomposites with mole fraction variations of the Mn of 0.25, 0.5, and 0.75. The crystalline phase of the synthesized MnxFe3–xO4/rGO nanocomposites formed an amorphous phase. The presence of rGO was observed through EDX results. The magnetical properties of MnxFe3–xO4/rGO nanocomposites were shown by decreasing the Br, HcJ, Hmax along with increasing of Mn doping. Interestingly, increasing rGO and Mn composition made the absorption bandwidth of the MnxFe3–xO4/rGO nanocomposites wider, so that the radar absorption also increased marking by the greater reflection loss that reached −11.95 dB. The increase in the radar absorption performance of MnxFe3–xO4/rGO nanocomposites came from the efficient complementarity between dielectric loss and magnetic loss and interfacial polarization between Fe3O4 doped Mn and rGO.

Open Access Research Article Issue
Fe-TiO2/zeolite H-A photocatalyst for degradation of waste dye (methylene blue) under UV irradiation
AIMS Materials Science 2023, 10(1): 40-54
Published: 15 February 2023
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Industrial wastewater contains non-biodegradable dyes that are highly toxic to humans and aquatic life. As solution from photocatalytic degradation, TiO2 is one of the effective photocatalysts for wastewater degradation, but it has low adsorption power. To overcome this deficiency, this study synthesized a new photocatalyst by Fe-TiO2/zeolite H-A. The photocatalyst was successfully synthesized by the impregnation method and was systematically characterized by XRD, XRF, SEM, FT-IR and UV-Vis DRS. XRD diffractogram at 2θ = 25.3° showed anatase phase of the photocatalyst. SEM results showed a rough and soft surface with a size of 491.49 nm. FT-IR analysis obtained the zeolite-A characteristic band, vibration of Ti-O-Ti groups and the vibration of the Fe-O group. The bandwidth of the band gap was 3.16 eV. The photocatalytic efficiency of methylene blue degradation reached 89.58% yield with optimum conditions: irradiation time of 50 min, pH 9 and concentration of methylene blue about 20 mg/L. Fe-TiO2/zeolite H-A as a new photocatalyst can be an alternative photocatalyst to purify methylene blue.

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