In-situ study of the microstructure evolution during tension of a Mg-Y-Zn-Al alloy processed by rapidly solidified ribbon consolidation technique

Mg-Y-Zn-Al alloys processed by rapidly solidified ribbon consolidation (RSRC) technique exhibit an exceptional mechanical performance indicating promising application potential. This material has a bimodal microstructure consisting of fine recrystallized and coarse non-recrystallized grains with solute-rich stacking faults forming cluster arranged layers (CALs) and nanoplates (CANaPs), or complete long period stacking ordered (LPSO) phase. In order to reveal the deformation mechanisms, in-situ synchrotron X-ray diffraction line profile analysis was employed for a detailed study of the dislocation arrangement created during tension in Mg - 0.9% Zn - 2.05% Y - 0.15% Al (at%) alloy. For uncovering the effect of the initial microstructure on the mechanical performance, additional samples were obtained by annealing of the as-consolidated specimen at 300 and 400 ℃ for 2 h. The heat treatment at 300 ℃ had no significant effect on the initial microstructure, its evolution during tension and, thus, the overall deformation behavior under tensile loading. On the other hand, annealing at 400 ℃ resulted in a significant increase of the recrystallized grains fraction and a decrease of the dislocation density, leading to only minor degradation of the mechanical strength. The maximum dislocation density at the failure of the samples corresponding to the plastic strain of 10–25% was estimated to be about 16–20 × 10¹⁴ m⁻². The diffraction profile analysis indicated that most dislocations formed during tension were of non-basal 〈a〉 and pyramidal 〈c + a〉 types, what was also in agreement with the Schmid factor values revealed independently from orientation maps. It was also shown that the dislocation-induced Taylor hardening was much lower below the plastic strain of 3% than above this value, which was explained by a model of the interaction between prismatic dislocations and CANaPs/LPSO plates.