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Dynamic friction occurs not only between two contact objects sliding against each other, but also between two relative sliding surfaces several nanometres apart. Many emerging micro- and nano-mechanical systems that promise new applications in sensors or information technology may suffer or benefit from noncontact friction. Herein we demonstrate the distance-dependent friction energy dissipation between the tip and the heterogeneous polymers by the bimodal atomic force microscopy (AFM) method driving the second order flexural and the first order torsional vibration simultaneously. The pull-in problem caused by the attractive force is avoided, and the friction dissipation can be imaged near the surface. The friction dissipation coefficient concept is proposed and three different contact states are determined from phase and energy dissipation curves. Image contrast is enhanced in the intermediate setpoint region. The work offers an effective method for directly detecting the friction dissipation and high resolution images, which overcomes the disadvantages of existing methods such as contact mode AFM or other contact friction and wear measuring instruments.


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Dynamic friction energy dissipation and enhanced contrast in high frequency bimodal atomic force microscopy

Show Author's information Xinfeng TANDan GUO( )Jianbin LUO( )
State Key Laboratory of Tribology, Tsinghua University, Beijing 100084, China

Abstract

Dynamic friction occurs not only between two contact objects sliding against each other, but also between two relative sliding surfaces several nanometres apart. Many emerging micro- and nano-mechanical systems that promise new applications in sensors or information technology may suffer or benefit from noncontact friction. Herein we demonstrate the distance-dependent friction energy dissipation between the tip and the heterogeneous polymers by the bimodal atomic force microscopy (AFM) method driving the second order flexural and the first order torsional vibration simultaneously. The pull-in problem caused by the attractive force is avoided, and the friction dissipation can be imaged near the surface. The friction dissipation coefficient concept is proposed and three different contact states are determined from phase and energy dissipation curves. Image contrast is enhanced in the intermediate setpoint region. The work offers an effective method for directly detecting the friction dissipation and high resolution images, which overcomes the disadvantages of existing methods such as contact mode AFM or other contact friction and wear measuring instruments.

Keywords: dynamic friction, energy dissipation, contact states, image contrast, bimodal atomic force microscopy (AFM)

References(62)

[1]
Urbakh M, Meyer E. NANOTRIBOLOGY The renaissance of friction. Nat Mater 9(1): 8-10 (2010)
[2]
Kisiel M, Gnecco E, Gysin U, Marot L, Rast S, Meyer E. Suppression of electronic friction on Nb films in the superconducting state. Nat Mater 10(2): 119-122 (2011)
[3]
Holmberg K, Erdemir A. Influence of tribology on global energy consumption, costs and emissions. Friction 5(3): 263-284 (2017)
[4]
Tan X, Luo J. Research Advances of Lubrication. China Mechanical Engineering 31(2): 145-174, 189 (2020)
[5]
Meng Y, Xu J, Jin Z, Prakash B, Hu Y. A review of recent advances in tribology. Friction 8(2): 221-300 (2020)
[6]
Binnig G, Quate C F, Gerber C. Atomic force microscope. Phys Rev Lett 56(9): 930-933 (1986)
[7]
Albrecht T R, Grutter P, Horne D, Rugar D. Frequency-modulation detection using high-Q cantilevers for enhanced force microscope sensitivity. J Appl Phys 69(2): 668-673 (1991)
[8]
Giessibl F J. Atomic resolution of the silicon (111)-(7x7) surface by atomic force microscopy. Science 267(5194): 68-71 (1995)
[9]
Herruzo E T, Asakawa H, Fukuma T, Garcia R. Three-dimensional quantitative force maps in liquid with 10 piconewton, angstrom and sub-minute resolutions. Nanoscale 5(7): 2678-2685 (2013)
[10]
Martin-Jimenez D, Chacon E, Tarazona P, Garcia R. Atomically resolved three-dimensional structures of electrolyte aqueous solutions near a solid surface. Nat Commun 7: 12164 (2016)
[11]
Ky D L C, Khac B C T, Le C T, Kim Y S, Chung K H. Friction characteristics of mechanically exfoliated and CVD-grown single-layer MoS2. Friction 6(4): 395-406 (2018)
[12]
Luo J, Zhou X. Superlubricitive engineering-Future industry nearly getting rid of wear and frictional energy consumption. Friction 8(4): 643-665 (2020)
[13]
Mate C M, McClelland G M, Erlandsson R, Chiang S. Atomic-scale friction of a tungsten tip on a graphite surface. Phys Rev Lett 59(17): 1942-1945 (1987)
[14]
Liu L, Zhou M, Jin L, Li L, Mo Y, Su G, Li X, Zhu H, Tian Y. Recent advances in friction and lubrication of graphene and other 2D materials: Mechanisms and applications. Friction 7(3): 199-216 (2019)
[15]
Liu S-W, Wang H-P, Xu Q, Ma T-B, Yu G, Zhang C, Geng D, Yu Z, Zhang S, Wang W, et al. Robust microscale superlubricity under high contact pressure enabled by graphene-coated microsphere. Nat Commun 8(1): 14029 (2017)
[16]
Wang W, Xie G, Luo J. Black phosphorus as a new lubricant. Friction 6(1): 116-142 (2018)
[17]
Giessibl F J, Herz M, Mannhart J. Friction traced to the single atom. Proc Natl Acad Sci USA 99(19): 12006-12010 (2002)
[18]
Weymouth A J, Meuer D, Mutombo P, Wutscher T, Ondracek M, Jelinek P, Giessibl F J. Atomic structure affects the directional dependence of friction. Phys Rev Lett 111(12): 126103 (2013)
[19]
Kawai S, Sasaki N, Kawakatsu H. Direct mapping of the lateral force gradient on Si(111)-7x7. Phys Rev B 79(19): 195412 (2009)
[20]
Naitoh Y, Turansky R, Brndiar J, Li Y J, Stich I, Sugawara Y. Subatomic-scale force vector mapping above a Ge(001) dimer using bimodal atomic force microscopy. Nat Phys 13(7): 663-667 (2017)
[21]
Umeda N, Ishizaki S, Uwai H. Scanning attractive force microscope using photothermal vibration. J Vac Sci Technol B 9(2): 1318-1322 (1991)
[22]
Nishida S, Kobayashi D, Sakurada T, Nakazawa T, Hoshi Y, Kawakatsu H. Photothermal excitation and laser Doppler velocimetry of higher cantilever vibration modes for dynamic atomic force microscopy in liquid. Rev Sci Instrum 79(12): 123703 (2008)
[23]
Tan X, Shi S, Guo D, Luo J. Dynamical characterization of micro cantilevers by different excitation methods in dynamic atomic force microscopy. Rev Sci Instrum 89(11): 115109 (2018)
[24]
Rodriguez T R, Garcia R. Compositional mapping of surfaces in atomic force microscopy by excitation of the second normal mode of the microcantilever. Appl Phys Lett 84(3): 449-451 (2004)
[25]
Lai C-Y, Santos S, Chiesa M. Systematic multidimensional quantification of nanoscale systems from bimodal atomic force microscopy data. Acs Nano 10(6): 6265-6272 (2016)
[26]
Shi S, Guo D, Luo J. Enhanced phase and amplitude image contrasts of polymers in bimodal atomic force microscopy. RSC Adv 7(19): 11768-11776 (2017)
[27]
Forchheimer D, Forchheimer R, Haviland D B. Improving image contrast and material discrimination with nonlinear response in bimodal atomic force microscopy. Nat Commun 6(1): 6270 (2015)
[28]
Shi S, Guo D, Luo J. Interfacial interaction and enhanced image contrasts in higher mode and bimodal mode atomic force microscopy. RSC Adv 7(87): 55121-55130 (2017)
[29]
Garcia R, Herruzo E T. The emergence of multifrequency force microscopy. Nat Nanotechnol 7(4): 217-26 (2012)
[30]
Nievergelt A P, Adams J D, Odermatt P D, Fantner G E. High-frequency multimodal atomic force microscopy. Beilstein J Nanotechnol 5: 2459-2467 (2014)
[31]
Platz D, Tholen E A, Pesen D, Haviland D B. Intermodulation atomic force microscopy. Appl Phys Lett 92(15): 153106 (2008)
[32]
Lai C-Y, Perri S, Santos S, Garcia R, Chiesa M. Rapid quantitative chemical mapping of surfaces with sub-2 nm resolution. Nanoscale 8(18): 9688-9694 (2016)
[33]
Athanasopoulou E-N, Nianias N, Ong Q K, Stellacci F. Bimodal atomic force microscopy for the characterization of thiolated self-assembled monolayers. Nanoscale 10(48): 23027-23036 (2018)
[34]
Benaglia S, Amo C A, Garcia R. Fast, quantitative and high resolution mapping of viscoelastic properties with bimodal AFM. Nanoscale 11(32): 15289-15297 (2019)
[35]
Shi S, Guo D, Luo J B. Imaging contrast and tip-sample interaction of non-contact amplitude modulation atomic force microscopy with Q-control. J Phys D-Appl Phys 50(41): 415307 (2017)
[36]
Kunstmann T, Schlarb A, Fendrich M, Paulkowski D, Wagner T, Moller R. Combined normal and torsional mode in frequency-modulation atomic force microscopy for lateral dissipation measurement. Appl Phys Lett 88(15): 153112 (2006)
[37]
Yurtsever A, Gigler A M, Dietz C, Stark R W. Frequency modulated torsional resonance mode atomic force microscopy on polymers. Appl Phys Lett 92(14): 143103 (2008)
[38]
Kawai S, Glatzel T, Koch S, Such B, Baratoff A, Meyer E. Ultrasensitive detection of lateral atomic-scale interactions on graphite (0001) via bimodal dynamic force measurements. Phys Rev B 81(8): 085420 (2010)
[39]
Dietz C. Sensing in-plane nanomechanical surface and sub-surface properties of polymers: local shear stress as function of the indentation depth. Nanoscale 10(1): 460-468 (2018)
[40]
Tan X, Guo D, Luo J. Different directional energy dissipation of heterogeneous polymers in bimodal atomic force microscopy. RSC Adv 9(47): 27464-27474 (2019)
[41]
Socoliuc A, Gnecco E, Maier S, Pfeiffer O, Baratoff A, Bennewitz R, Meyer E. Atomic-scale control of friction by actuation of nanometer-sized contacts. Science 313(5784): 207-210 (2006)
[42]
Lantz M A, Wiesmann D, Gotsmann B. Dynamic superlubricity and the elimination of wear on the nanoscale. Nat Nanotechnol 4(9): 586-591 (2009)
[43]
Shi S, Guo D, Luo J. Micro/atomic-scale vibration induced superlubricity. Friction 9(5): 1163-1174 (2021)
[44]
Forchheimer D, Forchheimer R, Haviland D B. Improving image contrast and material discrimination with nonlinear response in bimodal atomic force microscopy. Nat Commun 6(1): 6270 (2015)
[45]
Ding R-F, Yang C-W, Huang K-Y, Hwang I-S. High-sensitivity imaging with lateral resonance mode atomic force microscopy. Nanoscale 8(43): 18421-18427 (2016)
[46]
Egberts P, Ye Z J, Liu X Z, Dong Y L, Martini A, Carpick R W. Environmental dependence of atomic- scale friction at graphite surface steps. Phys Rev B 88(3): 035409 (2013)
[47]
Martinez N F, Garcia R. Measuring phase shifts and energy dissipation with amplitude modulation atomic force microscopy. Nanotechnology 17(7): S167-S172 (2006)
[48]
Sader J E, Chon J W M, Mulvaney P. Calibration of rectangular atomic force microscope cantilevers. Rev Sci Instrum 70(10): 3967-3969 (1999)
[49]
Lozano J R, Garcia R. Theory of multifrequency atomic force microscopy. Phys Rev Lett 100(7): 076102 (2008)
[50]
Santos S. Phase contrast and operation regimes in multifrequency atomic force microscopy. Appl Phys Lett 104(14): 143109 (2014)
[51]
Garcia R, Gomez C J, Martinez N F, Patil S, Dietz C, Magerle R. Identification of nanoscale dissipation processes by dynamic atomic force microscopy. Phys Rev Lett 97(1): 016103 (2006)
[52]
Garcia R, Tamayo J, San Paulo A. Phase contrast and surface energy hysteresis in tapping mode scanning force microsopy. Surf Interface Anal 27(5-6): 312-316 (1999)
DOI
[53]
Chawla G, Solares S D. Mapping of conservative and dissipative interactions in bimodal atomic force microscopy using open-loop and phase-locked-loop control of the higher eigenmode. Appl Phys Lett 99(7): 074103 (2011)
[54]
Lozano J R, Garcia R. Theory of phase spectroscopy in bimodal atomic force microscopy. Phys Rev B 79(1): 014110 (2009)
[55]
Cleveland J P, Anczykowski B, Schmid A E, Elings V B. Energy dissipation in tapping-mode atomic force microscopy. Appl Phys Lett 72(20): 2613-2615 (1998)
[56]
Gomez C J, Garcia R. Determination and simulation of nanoscale energy dissipation processes in amplitude modulation AFM. Ultramicroscopy 110(6): 626-633 (2010)
[57]
Chen N, Bhushan B. Morphological, nanomechanical and cellular structural characterization of human hair and conditioner distribution using torsional resonance mode with an atomic force microscope. J Microsc 220(2): 96-112 (2005)
[58]
San Paulo A, Garcia R. Amplitude, deformation and phase shift in amplitude modulation atomic force microscopy: a numerical study for compliant materials. Surf Sci 471(1-3): 71-79 (2001)
[59]
Israelachvili J N, Intermolecular and Surface Forces, 3rd Edition. San Diego: Elsevier Academic Press Inc, 2011.
DOI
[60]
Ashman K M, Bird C M, Zepf S E. Detecting bimodality in astronomical datasets. Astron J 108(6): 2348-2361 (1994)
[61]
Stifter T, Marti O, Bhushan B. Theoretical investigation of the distance dependence of capillary and van der Waals forces in scanning force microscopy. Phys Rev B 62(20): 13667-13673 (2000)
[62]
Burnham N A, Colton R J, Pollock H M. Interpretation issues in force microscopy. J Vac Sci Technol A-Vac Surf Films 9(4): 2548-2556 (1991)
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Publication history

Received: 24 September 2020
Revised: 20 December 2020
Accepted: 07 January 2021
Published: 12 March 2021
Issue date: May 2022

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© The author(s) 2021.

Acknowledgements

This research is financially supported by the National Natural Science Foundation of China (No. 51527901).

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