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Research Article | Open Access

Synthesis and formation mechanism of titanium lead carbide

C. LINGa, W. B. TIANa( ), P. ZHANGa, W. ZHENGa, Y. M. ZHANGb, Z. M. SUNa( )
Jiangsu Key Laboratory of Advanced Metallic Materials, School of Materials Science and Engineering, Southeast University, Nanjing 211189, China
Jiangsu Key Laboratory of Construction Materials, School of Materials Science and Engineering, Southeast University, Nanjing 211189, China
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Abstract

Ti2PbC was synthesized for the first time by pressureless reaction synthesis using Ti/Pb/TiC as starting materials at a heating rate of 2 ℃/min and holding at 1370 ℃ for 2 h in a tube furnace protected by Ar atmosphere. The effects of starting powders, heating rates, and holding temperatures on the formation of Ti2PbC were investigated. It was found that elementary mixture of Ti/Pb/C or higher heating rates fail to form Ti2PbC. The decreased lattice parameters in the synthesized Ti2PbC indicated the existence of Pb vacancies in the compound. A reaction mechanism was proposed to explain the formation of Ti2PbC.

Keywords

Ti2PbCMAX phasedifferential scanning calorimetry (DSC)thermal stability

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Journal of Advanced Ceramics
Volume 7 Issue 2,
June 2018
Pages 178-183
DOI: 10.1007/s40145-018-0269-1

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LING C, TIAN WB, ZHANG P, et al. Synthesis and formation mechanism of titanium lead carbide. Journal of Advanced Ceramics, 2018, 7(2): 178-183. https://doi.org/10.1007/s40145-018-0269-1

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Received: 08 December 2017
Revised: 14 March 2018
Accepted: 16 March 2018
Published: 17 April 2018
© The author(s) 2018

Open Access The articles published in this journal are distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made.