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Nano Research 2024, 17(3): 1666-1675 https://doi.org/10.1007/s12274-023-6350-2
Research Article | Issue | Published: 16 December 2023

Flexible regulation engineering of titanium nitride nanofibrous membranes for efficient electromagnetic microwave absorption in wide temperature spectrum

Show Author's Information Cuiping Li1,2,§,  Lu Zhang1,2,§,  Shuai Zhang2,  Qiqi Yu1,2,  Dan Li1,2,  Lei Zhang1,  Chunhong Gong1,2( ),  Jingwei Zhang2
Institute of Functional Polymer Composites, College of Chemistry and Molecular Sciences, Henan University, Kaifeng 475004, China
National & Local Joint Engineering Research Center for Applied Technology of Hybrid Nanomaterials, Henan University, Kaifeng 475004, China

§ Cuiping Li and Lu Zhang contributed equally to this work.

Keywords:
dielectric loss, electromagnetic microwave absorption, flexible titanium nitride nanofibrous membranes, local conductive loss, wide temperature spectrum
Topics:
Inorganic compounds
Cite this article:
Li C, Zhang L, Zhang S, et al. Flexible regulation engineering of titanium nitride nanofibrous membranes for efficient electromagnetic microwave absorption in wide temperature spectrum. Nano Research, 2024, 17(3): 1666-1675. https://doi.org/10.1007/s12274-023-6350-2
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Abstract Full text Electronic supplementary material About this article

Simultaneous development of well impedance matching and strong loss capability has become a mainstream method for achieving outstanding electromagnetic microwave absorption (EMWA) performances over wide temperature range. However, it is difficult to pursue both due to the mutual restraint of relationship between impedance matching and loss capability about temperature. Here, we propose a flexible regulation engineering of titanium nitride (TiN) nanofibrous membranes (NMs, TNMs), which could be distributed uniformly in the polydimethylsiloxane (PDMS) matrix and contributed to the formation of abundant local conductive networks, generating the local conductive loss and enhancing the loss ability of EMWs. Moreover, when the TNMs are used as functional units and dispersed in the matrix, the corresponding composites exhibit an outstanding anti-reflection effect on microwaves. As hoped, under the precondition of good impedance matching, local conductive loss and polarization loss together improve the loss capacity at room temperature, and polarization loss can compensate the local conductive loss to acquire effective dielectric response at elevated temperature. Benefiting from the reasonably synergistic loss ability caused by flexible regulation engineering, the corresponding composites exhibit the perfect EMWA performances in a wide temperature range from 298 to 573 K. This work not only elaborates the ponderable insights of independent membrane in the composition-structure-function connection, but also provides a feasible tactic for resolving coexistence of well impedance matching and strong loss capability issues in wide temperature spectrum.


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Electronic supplementary material
About this article

Flexible regulation engineering of titanium nitride nanofibrous membranes for efficient electromagnetic microwave absorption in wide temperature spectrum

Show Author's information Cuiping Li1,2,§, Lu Zhang1,2,§, Shuai Zhang2, Qiqi Yu1,2, Dan Li1,2, Lei Zhang1, Chunhong Gong1,2( ), Jingwei Zhang2
Institute of Functional Polymer Composites, College of Chemistry and Molecular Sciences, Henan University, Kaifeng 475004, China
National & Local Joint Engineering Research Center for Applied Technology of Hybrid Nanomaterials, Henan University, Kaifeng 475004, China

§ Cuiping Li and Lu Zhang contributed equally to this work.

Abstract

Simultaneous development of well impedance matching and strong loss capability has become a mainstream method for achieving outstanding electromagnetic microwave absorption (EMWA) performances over wide temperature range. However, it is difficult to pursue both due to the mutual restraint of relationship between impedance matching and loss capability about temperature. Here, we propose a flexible regulation engineering of titanium nitride (TiN) nanofibrous membranes (NMs, TNMs), which could be distributed uniformly in the polydimethylsiloxane (PDMS) matrix and contributed to the formation of abundant local conductive networks, generating the local conductive loss and enhancing the loss ability of EMWs. Moreover, when the TNMs are used as functional units and dispersed in the matrix, the corresponding composites exhibit an outstanding anti-reflection effect on microwaves. As hoped, under the precondition of good impedance matching, local conductive loss and polarization loss together improve the loss capacity at room temperature, and polarization loss can compensate the local conductive loss to acquire effective dielectric response at elevated temperature. Benefiting from the reasonably synergistic loss ability caused by flexible regulation engineering, the corresponding composites exhibit the perfect EMWA performances in a wide temperature range from 298 to 573 K. This work not only elaborates the ponderable insights of independent membrane in the composition-structure-function connection, but also provides a feasible tactic for resolving coexistence of well impedance matching and strong loss capability issues in wide temperature spectrum.

Keywords: dielectric loss, electromagnetic microwave absorption, flexible titanium nitride nanofibrous membranes, local conductive loss, wide temperature spectrum

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Publication history
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Acknowledgements

Publication history

Received: 04 November 2023
Revised: 17 November 2023
Accepted: 18 November 2023
Published: 16 December 2023
Issue date: March 2024

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© Tsinghua University Press 2023

Acknowledgements

Acknowledgements

Thanks for the financial support of the National Natural Science Foundation of China (Nos. 22305066 and U1704253).

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