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An arc-discharge method using a buffer gas containing carbon dioxide has been developed for the efficient and large-scale synthesis of few-layered graphene. The resulting samples of few-layered graphene, well-dispersed in organic solvents such as N, N-dimethylformamide (DMF) and 1, 2-dichlorobenzene (o-DCB), were examined by transmission electron microscopy (TEM), X-ray diffraction (XRD), Raman spectroscopy, atomic force microscopy (AFM), and thermal gravimetric analysis (TGA). The electrical conductivity and transparency of flexible films prepared using a direct solution process have also been studied.


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Efficient and Large-Scale Synthesis of Few-Layered Graphene Using an Arc-Discharge Method and Conductivity Studies of the Resulting Films

Show Author's information Yingpeng WuBin WangYanfeng MaYi HuangNa LiFan ZhangYongsheng Chen( )
Key Laboratory of Functional Polymer Materials and Center for Nanoscale Science & TechnologyInstitute of Polymer ChemistryCollege of ChemistryNankai UniversityTianjin300071China

Abstract

An arc-discharge method using a buffer gas containing carbon dioxide has been developed for the efficient and large-scale synthesis of few-layered graphene. The resulting samples of few-layered graphene, well-dispersed in organic solvents such as N, N-dimethylformamide (DMF) and 1, 2-dichlorobenzene (o-DCB), were examined by transmission electron microscopy (TEM), X-ray diffraction (XRD), Raman spectroscopy, atomic force microscopy (AFM), and thermal gravimetric analysis (TGA). The electrical conductivity and transparency of flexible films prepared using a direct solution process have also been studied.

Keywords: Graphene, conductivity, film, arc-discharge, few-layered

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Received: 10 May 2010
Revised: 29 June 2010
Accepted: 03 August 2010
Published: 09 September 2010
Issue date: September 2010

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© The Author(s) 2010

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Acknowledgements

The authors gratefully acknowledge financial support from the National Natural Science Foundation of China (NSFC) (Nos. 50933003, 20774047, 50903044, 50902073), the Chinese Ministry of Science and Technology (MOST) (No. 2009AA032304), and the Natural Science Foundation (NSF) of Tianjin Municipality (No. 08JCZDJC25300).

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