TY - JOUR AU - XIN, Xin AU - TAN, Zexin AU - ZHAO, Junxue AU - HU, Ailin AU - WANG, Ze AU - KANG, Yi AU - WANG, He AU - ZHANG, Zhenkai PY - 2022 TI - Heat Treatment Process Optimization of Microcrystalline Cast Stone from Silico-manganese Slag by One-Step Preparation JO - Journal of the Chinese Ceramic Society SN - 0454-5648 SP - 1677 EP - 1684 VL - 50 IS - 6 AB - Silico-manganese slag is a main solid waste produced from production of silicon-manganese alloy, which affects the environment. It is thus necessary to explore the corresponding disposal methods since the exsiting processing technology restricts the absorbing capacity. A microcrystalline cast stone was fabricated by the Petrurgic firing method with silico-manganese slag as a raw material. The bulk density, microhardness, flexural and compressive strength of the samples were determined. The influences of crystallization temperature and time on the phase structure and properties of the finished product were invesigated. The results show that a hot molten slag is cooled to 950 ℃ for 60 min and then annealed at 760 ℃ , obtaing a microcrystalline cast stone with the superior properties. The microcrystalline cast stone has a compact structure, and the precipitated crystal phases are mainly clinopyroxene, diopside and aluminum diopside, as well as anorthite and wollastonite. The bulk density of the cast stone can reach 3.11×103 kg·m–3, the microhardness is 8.77×103 MPa, and the flexural strength and the compressive strength are 86 MPa and 222.9 MPa, respectively. UR - https://doi.org/10.14062/j.issn.0454-5648.20210843 DO - 10.14062/j.issn.0454-5648.20210843