@article{Yang2024, 
author = {Siyi Yang and Jian Luo and Yinghui Xu and Mingjie Wu and Yingkui Yang},
title = {Oxygen evolution reaction performance misjudgment caused by the self-oxidation process},
year = {2024},
journal = {Nano Research Energy},
volume = {3},
pages = {e9120136},
keywords = {oxygen evolution reaction, electrochemical impedance spectroscopy, self-oxidation reaction, multi-potential step method},
url = {https://www.sciopen.com/article/10.26599/NRE.2024.9120136},
doi = {10.26599/NRE.2024.9120136},
abstract = {Based on the interference effect of surface self-oxidation peak on the oxygen evolution reaction (OER) performance, appropriate experimental strategies and data processing methods are crucial to correctly identify and address the oxidation peak in nickel-based materials to ensure data accuracy. Considering these facts that frequent OER performance misjudgment would confuse the readers, we revealed this reason and proposed the use of multi-potential step method to avoid non-steady-state currents caused by capacitive charging effects or intermediate oxidation. Additionally, combining electrochemical impedance spectroscopy (EIS) analysis, we discussed high-frequency response characteristics to further reveal the surface self-oxidation process. These research findings are crucial for accurately evaluating the actual performance of some special materials in electrochemical catalysis.}
}