TY - JOUR AU - Hong, Xufeng AU - He, Liang AU - Ma, Xinyu AU - Yang, Wei AU - Chen, Yiming AU - Zhang, Lei AU - Yan, Haowu AU - Li, Zhaohuai AU - Mai, Liqiang PY - 2017 TI - Microstructuring of carbon/tin quantum dots via a novel photolithography and pyrolysis-reduction process JO - Nano Research SN - 1998-0124 SP - 3743 EP - 3753 VL - 10 IS - 11 AB - A novel microfabrication process based on optimized photolithography combined with pyrolysis-reduction is proposed to fabricate interdigital porous carbon/tin quantum dots (C/Sn QDs) microelectrodes. C/Sn QDs active microelectrodes are also employed as current collectors of a micro-supercapacitor (MSC). A uniform dispersion of Sn QDs (diameter of ~3 nm) in the carbon matrix is achieved using our facile and controllable microfabrication process. The as-fabricated C/Sn QDs MSC obtained by carbonization at 900 ℃ exhibits a higher areal specific capacitance (5.79 mF·cm-2) than that of the pyrolyzed carbon-based MSC (1.67 mF·cm-2) and desirable cycling stability (93.3% capacitance retention after 5, 000 cyclic voltammetry cycles). This novel microfabrication process is fully compatible with micromachining technologies, showing great potential for large-scale fine micropatterning of carbon-based composites for applications in micro/nano devices. UR - https://doi.org/10.1007/s12274-017-1587-2 DO - 10.1007/s12274-017-1587-2