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Research Article | Open Access

Microstructure and mechanical properties of short-carbon-fiber/Ti3SiC2 composites

Guangqi HEa,bRongxiu GUOaMeishuan LIbYang YANGb,cLinshan WANGdYuhai QIANbJun ZUObJingjun XUb( )Changsheng LIUa( )
School of Materials Science and Engineering, Northeastern University, Shenyang 110819, China
Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
School of Materials Science and Engineering, University of Science and Technology of China, Shenyang 110016, China
College of Science, Northeastern University, Shenyang 110819, China
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Short-carbon-fibers (Csf) reinforced Ti3SiC2 matrix composites (Csf/Ti3SiC2, the Csf content was 0 vol%, 2 vol%, 5 vol%, and 10 vol%) were fabricated by spark plasma sintering (SPS) using Ti3SiC2 powders and Csf as starting materials at 1300 ℃. The effects of Csf addition on the phase compositions, microstructures, and mechanical properties (including hardness, flexural strength (σf), and KIC) of Csf/Ti3SiC2 composites were investigated. The Csf, with bi-layered transition layers, i.e., TiC and SiC layers, were homogeneously distributed in the as-prepared Csf/Ti3SiC2 composites. With the increase of Csf content, the KIC of Csf/Ti3SiC2 composites increased, but the σf decreased, and the Vickers hardness decreased initially and then increased steadily when the Csf content was higher than 2 vol%. These changed performances (hardness, σf, and KIC) could be attributed to the introduction of Csf and the formation of stronger interfacial phases.


MW Barsoum. The MN+1AXN phases: A new class of solids. Prog Solid State Chem 2000, 28: 201-281.
MW Barsoum, T El-Raghy. Synthesis and characterization of a remarkable ceramic: Ti3SiC2. J Am Ceram Soc 1996, 79: 1953-1956.
T El-Raghy, A Zavaliangos, MW Barsoum, et al. Damage mechanisms around hardness indentations in Ti3SiC2. J Am Ceram Soc 2005, 80: 513-516.
M Barsoum, T El-Raghy. A progress report on Ti3SiC2, Ti3GeC2, and the H-phases, M2BX. J Mater Synth Process 1997, 5: 197-216.
YC Zhou, ZM Sun, SQ Chen, et al. In-situ hot pressing/solid-liquid reaction synthesis of dense titanium silicon carbide bulk ceramics. Mater Res Innov 1998, 2: 142-146.
ZM Sun, YC Zhou, MS Li. Oxidation behaviour of Ti3SiC2-based ceramic at 900-1300 ℃ in air. Corros Sci 2001, 43: 1095-1109.
NF Gao, Y Miyamoto, D Zhang. Dense Ti3SiC2 prepared by reactive HIP. J Mater Sci 1999, 34: 4385-4392.
NC Ghosh, SP Harimkar. Phase analysis and wear behavior of in situ spark plasma sintered Ti3SiC2. Ceram Int 2013, 39: 6777-6786.
G Górny, M Rączka, L Stobierski, et al. Ceramic composite Ti3SiC2-TiB2—Microstructure and mechanical properties. Mater Charact 2009, 60: 1168-1174.
SB Li, JX Xie, LT Zhang, et al. Mechanical properties and oxidation resistance of Ti3SiC2/SiC composite synthesized by in situ displacement reaction of Si and TiC. Mater Lett 2003, 57: 3048-3056.
E Benko, P Klimczyk, S MacKiewicz, et al. cBN-Ti3SiC2 composites. Diam Relat Mater 2004, 13: 521-525.
WB Tian, ZM Sun, H Hashimoto, et al. Synthesis, microstructure and mechanical properties of Ti3SiC2-TiC composites pulse discharge sintered from Ti/Si/TiC powder mixture. Mater Sci Eng: A 2009, 526: 16-21.
HJ Wang, ZH Jin, Y Miyamoto. Effect of Al2O3 on mechanical properties of Ti3SiC2/Al2O3 composite. Ceram Int 2002, 28: 931-934.
SL Shi, W Pan. Toughening of Ti3SiC2 with 3Y-TZP addition by spark plasma sintering. Mater Sci Eng: A 2007, 447: 303-306.
LG Hou, RZ Wu, XD Wang, et al. Microstructure, mechanical properties and thermal conductivity of the short carbon fiber reinforced magnesium matrix composites. J Alloys compd 2017, 695: 2820-2826.
S Li, YM Zhang, JC Han, et al. Effect of carbon particle and carbon fiber on the microstructure and mechanical properties of short fiber reinforced reaction bonded silicon carbide composite. J Eur Ceram Soc 2013, 33: 887-896.
WH Hong, KX Gui, P Hu, et al. Preparation and characterization of high-performance ZrB2-SiC-Cf composites sintered at 1450 ℃. J Adv Ceram 2017, 6: 110-119.
MC Wang, ZG Zhang, ZJ Sun, et al. Effect of fiber type on mechanical properties of short carbon fiber reinforced B4C composites. Ceram Int 2009, 35: 1461-1466.
FY Yang, XH Zhang, JC Han, et al. Characterization of hot-pressed short carbon fiber reinforced ZrB2-SiC ultra-high temperature ceramic composites. J Alloys Compd 2009, 472: 395-399.
MA Lagos, C Pellegrini, I Agote, et al. Ti3SiC2-Cf composites by spark plasma sintering: Processing, microstructure and thermo-mechanical properties. J Eur Ceram Soc 2019, 39: 2824-2830.
C Tang, TH Li, JJ Gao, et al. Microstructure and mechanical behavior of the Cf/Ti3SiC2-SiC composites fabricated by compression molding and pressureless sintering. Ceram Int 2017, 43: 16204-16209.
XB Zhou, H Yang, FY Chen, et al. Joining of carbon fiber reinforced carbon composites with Ti3SiC2 tape film by electric field assisted sintering technique. Carbon 2016, 102: 106-115.
KX Gui, FY Liu, G Wang, et al. Microstructural evolution and performance of carbon fiber-toughened ZrB2 ceramics with SiC or ZrSi2 additive. J Adv Ceram 2018, 7: 343-351.
JQ Qin, DW He. Phase stability of Ti3SiC2 at high pressure and high temperature. Ceram Int 2013, 39: 9361-9367.
Z Sun, J Zhou, D Music, et al. Phase stability of Ti3SiC2 at elevated temperatures. Scr Mater 2006, 54: 105-107.
C Racault, F Langlais, R Naslain. Solid-state synthesis and characterization of the ternary phase Ti3SiC2. J Mater Sci 1994, 29: 3384-3392.
T El-Raghy, MW Barsoum. Diffusion kinetics of the carburization and silicidation of Ti3SiC2. J Appl Phys 1998, 83: 112-119.
NF Gao, Y Miyamoto, D Zhang. On physical and thermochemical properties of high-purity Ti3SiC2. Mater Lett 2002, 55: 61-66.
NC Ghosh, SP Harimkar. Microstructure and wear behavior of spark plasma sintered Ti3SiC2 and Ti3SiC2-TiC composites. Ceram Int 2013, 39: 4597-4607.
XW Yin, LF Cheng, LT Zhang, et al. Fibre-reinforced multifunctional SiC matrix composite materials. Int Mater Rev 2017, 62: 117-172.
JF Zhang, LJ Wang, W Jiang, et al. Effect of TiC content on the microstructure and properties of Ti3SiC2-TiC composites in situ fabricated by spark plasma sintering. Mater Sci Eng: A 2008, 487: 137-143.
S Karimirad, Z Balak. Characteristics of spark plasma sintered ZrB2-SiC-SCFs composites. Ceram Int 2019, 45: 6275-6281.
M Shahedi Asl. Microstructure, hardness and fracture toughness of spark plasma sintered ZrB2-SiC-Cf composites. Ceram Int 2017, 43: 15047-15052.
JJ Brennan, G McCarthy. Interfacial studies of refractory glass-ceramic-matrix/advanced-SiC-fiber-reinforced composites. Mater Sci Eng: A 1993, 162: 53-72.
XL He, YK Guo, ZM Yu, et al. Study on microstructures and mechanical properties of short-carbon-fiber-reinforced SiC composites prepared by hot-pressing. Mater Sci Eng: A 2009, 527: 334-338.
Y Arai, R Inoue, K Goto, et al. Carbon fiber reinforced ultra-high temperature ceramic matrix composites: A review. Ceram Int 2019, 45: 14481-14489.
CF Wang, L Chen, J Li, et al. Enhancing the interfacial strength of carbon fiber reinforced epoxy composites by green grafting of poly(oxypropylene) diamines. Compos Part A: Appl Sci Manuf 2017, 99: 58-64.
JF Sun, F Zhao, Y Yao, et al. High efficient and continuous surface modification of carbon fibers with improved tensile strength and interfacial adhesion. Appl Surf Sci 2017, 412: 424-435.
WS Yang, S Biamino, E Padovano, et al. Microstructure and mechanical properties of short carbon fibre/SiC multilayer composites prepared by tape casting. Compos Sci Technol 2012, 72: 675-680.
SQ Guo, CF Hu, H Gao, et al. SiC(SCS-6) fiber-reinforced Ti3AlC2 matrix composites: Interfacial characterization and mechanical behavior. J Eur Ceram Soc 2015, 35: 1375-1384.
Journal of Advanced Ceramics
Pages 716-725
Cite this article:
HE G, GUO R, LI M, et al. Microstructure and mechanical properties of short-carbon-fiber/Ti3SiC2 composites. Journal of Advanced Ceramics, 2020, 9(6): 716-725.








Web of Science






Received: 30 March 2020
Revised: 08 July 2020
Accepted: 13 July 2020
Published: 06 November 2020
© The Author(s) 2020

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