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Superconductor samples of type (CoFe2O4)xGdBa2Cu3O7-δ (0≤x≤0.1) were synthesized by the conventional solid-state reaction technique, whereas nanosized CoFe2O4 was prepared by co-precipitation method with grain size of about 8.5 nm. The elemental content of the prepared samples was determined using particle induced X-ray emission (PIXE). The temperature dependence of real ( χ) and imaginary ( χ) components of AC magnetic susceptibility (ACMS) at different magnetic field amplitude (3–15 Oe) was investigated. The analysis of the temperature dependence of ACMS was performed using Bean critical state model. The values of the critical current density Jc at T < Tp ( Tp is the inter-granular loss peak temperature) were calculated as a function of magnetic field and nanosized CoFe2O4 content. It was found that the low nanosized CoFe2O4 addition content (x = 0.01) improves the critical current density Jc of Gd-123 superconducting phase. The observed variation of Jc with temperature indicated that the weak links are changed from superconductor– normal metal–superconductor (SNS) for free sample to superconductor–insulator–superconductor (SIS) type of junctions for samples added with nanosized CoFe2O4 of x < 0.01. We also discussed the experimental results in the framework of the critical state model to estimate the effective volume fraction of the grains fg using Cole–Cole plots.


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The effect of nanosized CoFe2O4 addition on the magnetic properties of GdBa2Cu3O7-δ using AC magnetic susceptibility measurements

Show Author's information R. AWADa,b( )N. H. MOHAMMEDaA. I. ABOU ALYaS. ISBERcH. A. MOTAWEHdD. EL-SAID BAKEERdM. ROUMIÉe
Physics Department, Faculty of Science, Alexandria University, Alexandria, Egypt
Physics Department, American University of Beirut, Beirut, Lebanon
Physics Department, Faculty of Science, Damanhur University, Damanhur, Egypt
Accelerator Laboratory, Lebanese Atomic Energy Commission, Beirut, Lebanon
Physics Department, Faculty of Science, Beirut Arab University, Lebanon

Abstract

Superconductor samples of type (CoFe2O4)xGdBa2Cu3O7-δ (0≤x≤0.1) were synthesized by the conventional solid-state reaction technique, whereas nanosized CoFe2O4 was prepared by co-precipitation method with grain size of about 8.5 nm. The elemental content of the prepared samples was determined using particle induced X-ray emission (PIXE). The temperature dependence of real ( χ) and imaginary ( χ) components of AC magnetic susceptibility (ACMS) at different magnetic field amplitude (3–15 Oe) was investigated. The analysis of the temperature dependence of ACMS was performed using Bean critical state model. The values of the critical current density Jc at T < Tp ( Tp is the inter-granular loss peak temperature) were calculated as a function of magnetic field and nanosized CoFe2O4 content. It was found that the low nanosized CoFe2O4 addition content (x = 0.01) improves the critical current density Jc of Gd-123 superconducting phase. The observed variation of Jc with temperature indicated that the weak links are changed from superconductor– normal metal–superconductor (SNS) for free sample to superconductor–insulator–superconductor (SIS) type of junctions for samples added with nanosized CoFe2O4 of x < 0.01. We also discussed the experimental results in the framework of the critical state model to estimate the effective volume fraction of the grains fg using Cole–Cole plots.

Keywords: critical current density, Gd-123 phase, nanosized CoFe2O4, AC magnetic susceptibility (ACMS), particle induced X-ray emission (PIXE)

References(45)

[1]
Muralidhar M, Jirsa M, Sakai N, et al. Current progress in ternary LREBa2Cu3Oy materials and their application. Mat Sci Eng B 2008, 151: 90–94.
[2]
Sakai N, Lee S, Chikumoto N, et al. Delamination behavior of Gd123 coated conductor fabricated by PLD. Physica C 2011, 471: 1075–1079.
[3]
Xu C, Hu A, Ichihara M, et al. Enhanced flux pinning of air-processed Gd123 by doping ZrO2 nanoparticles. Physica C 2007, 460–462: 1341–1342.
[4]
Xu C, Hu A, Sakai N, et al. Flux pinning properties and superconductivity of Gd-123 superconductor with addition of nanosized SnO2/ZrO2 particles. Physica C 2006, 445–448: 357–360.
[5]
Xu Y, Hu A, Xu C, et al. Effect of ZrO2 and ZnO nanoparticles inclusions on superconductive properties of the melt-processed GdBa2Cu3O7−δ bulk superconductor. Physica C 2008, 468: 1363–1365.
[6]
Zhang YF, Izumi M, Li YJ, et al. Enhanced JC in air-processed GdBa2Cu3O7−δ superconductor bulk grown by the additions of nano-particles. Physica C 2011, 471: 840–842.
[7]
Abou Aly AI, Mohammed NH, Awad R, et al. Determination of superconducting parameters of GdBa2Cu3O7−δ added with nanosized ferrite CoFe2O4 from excess conductivity analysis. J Supercond Nov Magn 2012, 25: 2281–2290.
[8]
Xu Y, Izumi M, Zhang YF, et al. Enhancement of critical current density in Gd123 bulk superconductor doped with magnetic powder. Physica C 2009, 469: 1215–1217.
[9]
Zhang YF, Izumi M, Xu Y, et al. Enhanced performance in bulk superconductor GdBa2Cu3O7-δ with additions of α-Fe2O3 particles. J Phys: Conf Ser 2010, 234: 012052.
[10]
Awad R, Abou-Aly AI, Ibrahim IH, et al. Superconducting properties of zinc substitution in Tl-2223 phase. J Alloys Compd 2008, 460: 500–506.
[11]
Çelebi S. Comparative AC susceptibility analysis on Bi–(Pb)–Sr–Ca–Cu–O high-Tc superconductors. Physica C 1999, 316: 251–256.
[12]
Lee CY, Kao YH. Low-field magnetic susceptibility studies of high-Tc superconductors. Physica C 1995, 241: 167–180.
[13]
Yamada N, Akune T, Sakamoto N, et al. Temperature dependence of irreversibility fields in Re doped Hg-1223 superconductors. Physica C 2004, 412–414: 425–429.
[14]
Wimbush SC, Yu R, Bali R, et al. Addition of ferromagnetic CoFe2O4 to YBCO thin films for enhanced flux pinning. Physica C 2010, 470: S223–S224.
[15]
Mumtaz M, Naeem S, Nadeem K, et al. Study of nano-sized (ZnFe2O4)y particles/CuTl-1223 superconductor composites. Solid State Sci 2013, 22: 21–26.
[16]
Awad R, Abou Aly AI, Mohammed NH. Physical and mechanical properties of GdBa2Cu3O7−δ added with nanosized CoFe2O4. J Supercond Nov Magn 2014, 27: 1757–1767.
[17]
Abou Aly AI, Mohammed NH, Awad R, et al. Magneto-conductivity analysis for GdBa2Cu3O7−δ added with nanosized ferrite CoFe2O4. J Supercond Nov Magn 2013, 26: 2419–2428.
[18]
Roumié M, Nsouli B, Zahraman K, et al. First accelerator based ion beam analysis facility in Lebanon: Development and applications. Nucl Instr Meth B 2004, 219–220: 389–393.
[19]
Harrison JF, Eldred RA. Adv X-ray Anal 1973, 17: 560–569.
DOI
[20]
Nejedly Z, Campbell JL, Gama S. An Excel utility for the rapid characterization of “funny filters” in PIXE analysis. Nucl Instr Meth B 2004, 219–220: 136–139.
[21]
Maxwell JA, Teesdale WJ, Campbell JL. The Guelph PIXE software package II. Nucl Instr Meth B 1995, 95: 407–421.
[22]
Namuco SB, Lao ML, Sarmago RV. Granular responses of GdBa2Cu3O7-δ using ac magnetic susceptibility measurement under ac and dc magnetic fields. Physics Procedia 2013, 45: 169–172.
[23]
Awad R, Abou-Aly AI, Mahmoud SA, et al. Normal-state conduction mechanisms in GdBa2Cu3−xRuxO7−δ superconducting phase. J Supercond Nov Magn 2011, 24: 2227.
[24]
Mohanta A, Behera D. Effect of granularity and inhomogeneity in excess conductivity of YBa2Cu3O7−δ+ xBaTiO3 superconductor. Physica B 2011, 406: 877–884.
[25]
Amira A, Bouaicha F, Boussouf N, et al. Substitution of Sr2+ by Eu3+ in Bi-2201 ceramics, effects on structure and physical properties. Solid State Sci 2010, 12: 699–705.
[26]
Sedky A, Youssif MI. Correlation between superconducting volume fraction and critical current density in copper oxide superconducting systems. Physica C 2004, 403: 297–303.
[27]
Wang XL, Horvat J, Gu GD, et al. Enhanced flux pinning by Fe point defects in Bi2Sr2Ca(Cu1−xFex)2O8+δ single crystals. Physica C 2000, 337: 221–224.
[28]
Xu Y, Izumi M, Tsuzuki K, et al. Flux pinning properties in a GdBa2Cu3O7−δ bulk superconductor with the addition of magnetic alloy particles. Supercond Sci Technol 2009, 22: 095009
[29]
Bahgat AA, Shaisha EE, Saber MM. Study of microstructure and magnetic properties in copper oxide superconducting systems through AC magnetic susceptibility. Physica B 2007, 399: 70–76.
[30]
Ilonca G, Pop AV, Yang T-R, et al. Transport properties and ac susceptibility of (Bi1.6Pb0.4)Sr2Ca2Cu1−xCox)3Oy superconductors. Int J Inorg Mater 2001, 3: 763–767.
[31]
Huth M, Schmitt M, Adrain H. Influence of composition and long term annealing on the weak link behaviour of the high-Tc superconductor (Bi,Pb)2+xSr2−yCa2+yCu3+zO10+δ. Physica C1991, 178: 203–212.
[32]
Müller K-H, MacFarlane JC, Driver R. Josephson vortices and flux penetration in high temperature superconductors. Physica C 1989, 158: 69–75.
[33]
Gömöry F. Characterization of high-temperature superconductors by AC susceptibility measurements. Supercond Sci Technol 1997, 10: 523
[34]
Sedky A, Youssif MI, Khalil SM, et al. On the correlation between order parameter, superconducting volume fraction and critical current density in R:123 superconductors. Solid State Commun 2006, 139: 126–131.
[35]
Salamati H, Kameli P. Effect of deoxygenation on the weak-link behavior of YBa2Cu3O7−δ superconductors. Solid State Commun 2003, 125: 407–411.
[36]
Bean CP. Magnetization of high-field superconductors. Rev Mod Phys 1964, 36: 31
[37]
Sedky A, Youssif MI. Low-field AC susceptibility study of critical current density in Eu:123 and Bi:2223 superconductors. J Magn Magn Mater 2001, 237: 22–26.
[38]
Murphy SD, Renouard K, Crittenden R, et al. AC susceptibility of sintered high Tc superconductors—Bean’s model and shielding current. Solid State Commun 1989, 69: 367–371.
[39]
Lee MW, Tai MF, Luo SC, et al. Critical current densities in K3C60/Rb3C60 powders determined from AC/DC susceptibility measurements. Physica C 1995, 245: 6–11
[40]
De Gennes PG. Boundary effects in superconductors. Rev Mod Phys 1964, 36: 225.
[41]
Ambegaokar V, Baratoff A. Tunneling between superconductors. Phys Rev Lett 1963, 10: 486
[42]
Farbod M, Batvandi MR. Doping effect of Ag nanoparticles on critical current of YBa2Cu3O7−δ bulk superconductor. Physica C 2011, 471: 112–117.
[43]
Clem JR. Granular and superconducting-glass properties of the high-temperature superconductors. Physica C 1988, 153: 50–55.
[44]
Müller K-H. AC susceptibility of high temperature superconductors in a critical state model. Physica C 1989, 159: 717–726.
[45]
Cho JH. Linear and nonlinear susceptibilities of a Bi2Sr2CaCu2O8 single crystal with isotropic columnar defects. Physica C 2001, 361: 99–106.
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Publication history

Received: 28 September 2015
Accepted: 03 December 2015
Published: 31 March 2016
Issue date: June 2021

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© The author(s) 2016

Acknowledgements

This work was performed in the Superconductivity and Metallic-Glass Lab, Physics Department, Faculty of Science, Alexandria University, Alexandria, Egypt, in cooperation with the Accelerator Laboratory, Lebanese Atomic Energy Commission, CNRS, Beirut, Lebanon, and the American University of Beirut, Beirut, Lebanon.

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