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Nano Research 2022, 15(6): 5601-5609 https://doi.org/10.1007/s12274-022-4358-7
Research Article | Issue | Published: 18 April 2022

Multifunctional Ti3C2Tx-(Fe3O4/polyimide) composite films with Janus structure for outstanding electromagnetic interference shielding and superior visual thermal management

Show Author's Information Yali Zhang,  Zhonglei Ma,  Kunpeng Ruan,  Junwei Gu( )
Shaanxi Key Laboratory of Macromolecular Science and Technology, School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’ an 710072, China
Keywords:
electromagnetic interference shielding, photothermal conversion, Janus structure, Ti3C2Tx-(Fe3O4/PI) composite films , electrothermal conversion
Topics:
Conductive films
Cite this article:
Zhang Y, Ma Z, Ruan K, et al. Multifunctional Ti3C2Tx-(Fe3O4/polyimide) composite films with Janus structure for outstanding electromagnetic interference shielding and superior visual thermal management. Nano Research, 2022, 15(6): 5601-5609. https://doi.org/10.1007/s12274-022-4358-7
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Abstract Full text Electronic supplementary material About this article

Flexible multifunctional polymer-based electromagnetic interference (EMI) shielding composite films have important application values in the fields of 5G communication technology, wearable electronic devices and artificial intelligence. In this work, Fe3O4/polyamic acid (PAA) nanofiber films are prepared by in-situ polymerization and electrospinning technology, and Ti3C2Tx nanosheets are deposited on the surface of the Fe3O4/PAA nanofiber films via vacuum-assisted filtration. Then, Janus Ti3C2Tx-(Fe3O4/polyimide (PI)) composite films are obtained by thermal imidization. The two sides of the Janus films exhibit completely different properties. The Fe3O4/PI side has excellent hydrophobicity and insulation property, and the Ti3C2Tx side has hydrophilicity and terrific conductivity. When the mass fraction of Ti3C2Tx is 80 wt.%, the Janus Ti3C2Tx-(Fe3O4/PI) composite film has excellent EMI shielding performances and mechanical properties, with EMI shielding effectiveness, tensile strength and Young’s modulus reaching 66 dB, 114.5 MPa and 5.8 GPa, respectively. At the same time, electromagnetic waves show different absorption shielding effectiveness (SEA) when incident from two sides of the Janus films. When the electromagnetic waves are incident from the Fe3O4/PI side, the SEA of the Janus film is 58 dB, much higher than that when the electromagnetic waves are incident from the Ti3C2Tx side (39 dB). In addition, the Ti3C2Tx side of the Janus Ti3C2Tx-(Fe3O4/PI) composite films also has excellent electrothermal and photothermal conversion performances. When the applied voltage is 4 V, the stable surface temperature reaches 108 °C; when it is irradiated by simulated sunlight with power density of 200 mW/cm2, the stable surface temperature reaches 95 °C.


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Electronic supplementary material
About this article

Multifunctional Ti3C2Tx-(Fe3O4/polyimide) composite films with Janus structure for outstanding electromagnetic interference shielding and superior visual thermal management

Show Author's information Yali Zhang, Zhonglei Ma, Kunpeng Ruan, Junwei Gu( )
Shaanxi Key Laboratory of Macromolecular Science and Technology, School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi’ an 710072, China

Abstract

Flexible multifunctional polymer-based electromagnetic interference (EMI) shielding composite films have important application values in the fields of 5G communication technology, wearable electronic devices and artificial intelligence. In this work, Fe3O4/polyamic acid (PAA) nanofiber films are prepared by in-situ polymerization and electrospinning technology, and Ti3C2Tx nanosheets are deposited on the surface of the Fe3O4/PAA nanofiber films via vacuum-assisted filtration. Then, Janus Ti3C2Tx-(Fe3O4/polyimide (PI)) composite films are obtained by thermal imidization. The two sides of the Janus films exhibit completely different properties. The Fe3O4/PI side has excellent hydrophobicity and insulation property, and the Ti3C2Tx side has hydrophilicity and terrific conductivity. When the mass fraction of Ti3C2Tx is 80 wt.%, the Janus Ti3C2Tx-(Fe3O4/PI) composite film has excellent EMI shielding performances and mechanical properties, with EMI shielding effectiveness, tensile strength and Young’s modulus reaching 66 dB, 114.5 MPa and 5.8 GPa, respectively. At the same time, electromagnetic waves show different absorption shielding effectiveness (SEA) when incident from two sides of the Janus films. When the electromagnetic waves are incident from the Fe3O4/PI side, the SEA of the Janus film is 58 dB, much higher than that when the electromagnetic waves are incident from the Ti3C2Tx side (39 dB). In addition, the Ti3C2Tx side of the Janus Ti3C2Tx-(Fe3O4/PI) composite films also has excellent electrothermal and photothermal conversion performances. When the applied voltage is 4 V, the stable surface temperature reaches 108 °C; when it is irradiated by simulated sunlight with power density of 200 mW/cm2, the stable surface temperature reaches 95 °C.

Keywords: electromagnetic interference shielding, photothermal conversion, Janus structure, Ti3C2Tx-(Fe3O4/PI) composite films , electrothermal conversion

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Publication history
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Acknowledgements

Publication history

Received: 16 March 2022
Revised: 23 March 2022
Accepted: 24 March 2022
Published: 18 April 2022
Issue date: April 2022

Copyright

© Tsinghua University Press 2022

Acknowledgements

The authors are grateful for the supports from the National Natural Science Foundation of China (Nos. U21A2093 and 51903145), Fundamental Research Funds for the Central Universities (No. D5000210627). Y. L. Z. would like to thank the Innovation Foundation for Doctor Dissertation of Northwestern Polytechnical University (No. CX2021107). This work is also financially supported by Polymer Electromagnetic Functional Materials Innovation Team of Shaanxi Sanqin Scholars.

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