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MIL-101(Cr) is a promising moisture absorbent for solar-driven waterharvesting from moisture to tackle the worldwide water shortage issue.However, the MIL-101(Cr) powder suffers from a long ab/desorption cycledue to the crystal aggregation caused by its inherent powder properties.Here, we demonstrate a MIL-101(Cr) nanofibrous composite membrane witha nanofibrous matrix where MIL-101(Cr) is monodisperse in the 3D porousnanofibrous matrix through a simple spray-electrospinning strategy. Thecontinuous porous nanofibrous matrix not only offers sufficient sites for MIL-101(Cr) loading but also provides rapid moisture transport channels,resulting in a super-rapid ab/desorption duration of 50 min (including anabsorption process for 40 min and a desorption process for 10 min) andmulticycle daily water production of 15.9 L kg−1 d−1. Besides, the MIL-101 (Cr) nanofibrous composite membrane establishes a high solar absorption of 92.8%, and excellent photothermal conversion with the surface temperature of 70.7 °C under one-sun irradiation. In addition, the MIL-101(Cr) nanofibrous composite membrane shows excellent potential for practical application due to its flexibility, portability, and use stability. This work provides a new perspective of shortening MOF ab/desorption duration by introducing a porous nanofibrous matrix to improve the specific water production for the solar-driven ab/desorption water harvesting technique.
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